OPTIMASI KINERJA ANALITIK PADA PENENTUAN KADAR FOSFOR SEBAGAI P2O5 PADA ABU BATUBARA DENGAN METODE SPEKTROFOTOMETER VISIBLE

  • Eka Apriska S Kusuma Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman
  • Aman Sentosa Panggabean Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman
  • Yasser Arafat Jurusan Kimia Fakultas Matematika dan Ilmu Pengetahuan Alam Universitas Mulawarman

Abstract

The research on optimization of analytical performance in the determination of phosphorous as P2O5 content in the coal ash with visible spectrophotometer method has been done. In this research was conducted validation visible spectrophotometer method to establish the levels of phosphorus in coal ash. Validation parameters used in this research were accuracy, precision, linearity, LOD, LOQ and ruggedness methods. From the result of this research, accuracy was stated in percent recovery, precision was stated as a RSD percent, withthe equation of linearity as y=0,1768x - 0,0076. From the equation, it will be obtained LOD and LOQ values. And endurance test methods that varied the length of it digest time. From the results it can be concluded that the determination of phosphorous content in the coal ash using visible spectrophotometer method has good precisionand accuracy, and able to be justified

Keywords: Coal, Phosporous, Analytical Performance, Visible Spectrophotometer.

Downloads

Download data is not yet available.

References

Akhadi, M. 2000. Listrik Mudah atau Udara Bersih. Elektro Indonesia.

Anonim. 2014. Prosedur Kerja dan Pemeliharaan Spektrofotometri Samarinda: PT.Geoservices Samarinda.

Budi, P. 1999. Kumpulan Makalah, Kolokium Pemutakhiran Ilmu Kimia. Laboratorium Kimia Radiasi. Fakultas MIPA UNHAS. Makassar.

Green, M. J. 1996. A Practical Guide to Analytical Method Validation Anal. Chein, News and Feature, May 1, Hal 305 A-309A.

Sukandarrumidi. 2008. Batu Bara dan Gambut. Universitas Gadjah Mada Press. Yogyakarta.

Sumardi, 2004. Uji Kinerja (Validasi) Metode Analisis Petunjuk Umum. RC Chem Learning Centre.Bandung.
Published
2016-01-19
How to Cite
KUSUMA, Eka Apriska S; PANGGABEAN, Aman Sentosa; ARAFAT, Yasser. OPTIMASI KINERJA ANALITIK PADA PENENTUAN KADAR FOSFOR SEBAGAI P2O5 PADA ABU BATUBARA DENGAN METODE SPEKTROFOTOMETER VISIBLE. JURNAL KIMIA MULAWARMAN, [S.l.], v. 13, n. 1, jan. 2016. ISSN 2476-9258. Available at: <http://jurnal.kimia.fmipa.unmul.ac.id/index.php/JKM/article/view/37>. Date accessed: 24 apr. 2024.
Citation Formats
Issue
Vol 13 No 1 (2015)
Section
Artikel

Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.

Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal.

This license requires that reusers give credit to the creator. It allows reusers to distribute, remix, adapt, and build upon the material in any medium or format, even for commercial purposes. If others remix, adapt, or build upon the material, they must license the modified material under identical terms.

  • BY: Credit must be given to you, the creator.
  • SA: Adaptations must be shared under the same terms.

    •