SINTESIS SILIKA MESOPORI TERSULFONASI DARI ABU SEKAM PADI (Oryza sativa L.)
Abstract
A study on the synthesis of sulphonated mesoporous silica from rice husk ash (Oryza sativa L.) been conducted. The preparation of sulphonated MSU-H was conducted by several steps namely, extraction of silica from rice husk ash, synthesis of mesoporous silica, synthesis of sulphonated mesoporous silica with post-grafting method. The N2 adsorption-desorption characterization results show the surface area of mesoporous silica 134 m2/g, pore volume 0.81 cm3/g and pore size 24.13 nm. The FT-IR characterization results of sulphonated mesoporous silica indicate the presence of Si-O-Si, Si-O, O-H and C-H alkane clusters.
Keyword
Rice husk ash,, Mesoporous Silica,, Sulphonated,, Post-Grafting Method
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References
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[2] Coniwanti, P., R. Srikandhy, and Apriliyanni. 2008. Pengaruh proses pengeringan, normalitas HCl, dan temperatur pembakaran pada pembuatan silika dari sekam padi. Jurnal Teknik Kimia 15.
[3] Anggoro, D. D. 2005. Aktivitas dan Pemodelan Katalis Silikat dari Abu Sekam Padi untuk Konversi Heksana. Reaktor 9: 1-7.
[4] Pirez, C., A. F. Lee, J. C. Manayil, C. M. A. Parlett, and K. Wilson. 2014. Hydrothermal saline promoted grafting: a route to sulfonic acid SBA-15 silica with ultra-high acid site loading for biodiesel synthesis. Green Chemistry 16: 4506-4509.
[5] Ishizaki, K. 1998. Porous Material Process Technology and Application. Dordecht: Kluwer Academic Publishers.
[6] Hamdan, H. 1992. Introduction of Zeolites: Synthesis, Characterization and Modification. Malaysia: University Teknology Malaysia.
[7] Hadi, S. 1986. Metodologi Research. Yogyakarta: Andi Offset.
[8] Brunauer, S., Emmet, P.H., Teller, E. 1938. Adsorption of Gases in Multimolecular Layers. 60 (2), pp 309-319.
[9] Ulfa, M. 2016. Karakterisasi SAXRD, Adsorpsi-Desorpsi N2 dan TEM pada Karbon Mesopori dari Gelatin Tulang Sapi. Surakarta: Universitas Sebelas Maret.
[10] Gregg, S.J dan Sing, K.S.W. 1982. Adsorption, Surface Area and Porosity 2nd Edition. London: Academic Press.
[11] Bae, Jung A., Hwang, Seong Hee, Song, Ki Chang, Ko, Soo Young, Yim, Jin Heong. 2010. Syinthesis of Functionalized Mesoporous Material with Various Organo- Silanes. USA: American Scientific Publisher.
[12] Margolese, D., J. A. Melero, S. C. Christiansen, B. F. Chmelka, and G. D. Stucky. 2000. Direct Syntheses of Ordered SBA-15 Mesoporous Silica Containing Sulfonic Acid Groups. Chemistry of Materials 12: 2448-2459.
[13] Bibi, A., Ju, Huanxian. 2016. Effiction Enrichment of Glycopeptides with Sulfonic Acid-Functionalized Mesoporous Silica. 161:681-685.
Published
2018-08-28
How to Cite
MAYLINA, Ajeng Chandra; SUBAGYONO, R.R. Dirgarini Julia Nurlianti; DANIEL, Daniel.
SINTESIS SILIKA MESOPORI TERSULFONASI DARI ABU SEKAM PADI (Oryza sativa L.).
JURNAL ATOMIK, [S.l.], v. 3, n. 2, p. 73-78, aug. 2018.
ISSN 2549-0052.
Available at: <https://jurnal.kimia.fmipa.unmul.ac.id/index.php/JA/article/view/526>. Date accessed: 12 may 2025.
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